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EM-Tec transmission-EBSD sample holders for TEM and FIB grids
to generate transmission Kikuchi patterns




                                    
EM-Tec transmission-EBSD sample holders for TEM and FIB grids
Transmission-EBSD or t-EBSD  EBSD
Introduction

EBSD  analysis is a powerful microstructural crystallographic characterisation technique for crystalline or polycrystalline materials. Standard EBSD analysis on bulk samples and surfaces is performed on high-tilt samples (typically 70° from horzontal). The EBSD pattern reveals the crystal orientation and in polycrystalline materials the variation of orientation amongst the crystals. For optimum EBSD results, deformation free, polished surfaces are needed.

Transmission EBSD analysis is only possible on (very ) thin TEM samplessuspended on a TEM grid or on a TEM lamella attached to an FIB grid. EBSD analysis on thin samples can be performed in backscatter mode at 70° tilt (from horizontal) or transmision mode at 20° (from horizontal). For transmission EBSD or t-EBSD is is imperative that transmitted electrons can reach the EBSD detector without any obstruction.

The EM-Tec  t-EBSD holders are specifically designed to generate transmission Kikuchi patterns. The transmission EBSD holders include an opening of Ø2mm in the base. The top is formed by a fork-shaped phosphor bronze clip which clamps the TEM or FIB grid.  Transmission EBSD imaging and analysis is possible over the Ø2mm  area.
The  EM-Tec t-EBSD holders are available  with 1 of 3 TEM grid capacity. The choice of configuations include:

  • EM-Tec T1 t-EBSD sample holder for a single TEM or FIB grid, standard Ø3.2mm (1/8”) pin to be mounted on existing pre-tilt holders
  • EM-Tec T3 t-EBSD sample holder for three TEM or FIB grids, standard Ø3.2mm (1/8”) pin to be mounted on existing pre-tilt holders
  • EM-Tec TE1 t-EBSD sample holder kit for a single TEM or FIB grid with 70° and 20° pre-tilt, pin / M4
  • EM-Tec TE3 t-EBSD sample holder kit for three TEM or FIB grid with 70° and 20° pre-tilt, pin / M4

 

Capacity, size and compatibility of the EM-Tec t-EBSD sample holder and kits

Product #

Style

Tilt angles

Size w/o pin

TEM Grid Capacity

Compatibility

12-002371

EM-Tec T1

–    t-EBSD

6x11x4.5mm

1

3.2mm pin stub

12-002373

EM-Tec T3

–    t-EBSD

16x11x4.5mm

3

3.2mm pin stub

12-0002271

EM-Tec TE1

70° /20° t-EBSD

Ø12.7 x 30mm

1

3.2mm pin stub

12-0002273

EM-Tec TE3

70° /20° t-EBSD

Ø12.7 x 30mm

3

3.2mm pin stub

12-0003371

EM-Tec TE1

70° /20° t-EBSD

Ø12.7 x 30mm

1

M4 thread

12-0003373

EM-Tec TE3

70° /20° t-EBSD

Ø12.7 x 30mm

3

M4 thread


Ordering Information for EM-Tec t-EBSD sample holders to be mounted on existing pre-tilt holders. Compatible with SEMs using pin stubs; FEI, Philips, Zeiss, LEO, Tescan, AmRay, Cambridge Instruments, Leica, and CamScan.

*Prices are without tax. Tax might be added in cart.


EM-Tec TE3 t-EBSD holder for three TEM / FIB Lift-out grids, pin EM-Tec TE3 t-EBSD holder for three TEM / FIB Lift-out grids, pin
Product # Unit Price* Add to Quote / Cart
12-002373 each €450,00
Qty:



EM-Tec TE1 t-EBSD holder for a single TEM / FIB Lift-out grid, pin EM-Tec TE1 t-EBSD holder for a single TEM / FIB Lift-out grid, pin
Product # Unit Price* Add to Quote / Cart
12-002371 each €295,50
Qty:



3x EM-Tec replacement TEM grid clips for EM-Tec t-EBSD holders plus 3 x M2x3mm brass screw 3x EM-Tec replacement TEM grid clips for EM-Tec t-EBSD holders plus 3 x M2x3mm brass screw
Product # Unit Price* Add to Quote / Cart
12-002270 pkg/3 €75,00
Qty:


Ordering Information for EM-Tec t-EBSD sample holder kits with 20° / 70° pre-tilt angle for SEMs using pin stubs; FEI, Philips, Zeiss, LEO, TESCAN, AmRay, Cambridge Instruments, Leica, and CamScan.

*Prices are without tax. Tax might be added in cart.


EM-Tec TE3 t-EBSD holder kit 20 / 70 for three TEM / FIB Lift-out grid, pin EM-Tec TE3 t-EBSD holder kit 20 / 70 for three TEM / FIB Lift-out grid, pin
Product # Unit Price* Add to Quote / Cart
12-002273 each €482,50
Qty:



EM-Tec TE1 t-EBSD holder kit 20 / 70 for single TEM / FIB Lift-out grid, pin EM-Tec TE1 t-EBSD holder kit 20 / 70 for single TEM / FIB Lift-out grid, pin
Product # Unit Price* Add to Quote / Cart
12-002271 each €327,50
Qty:


Ordering Information for EM-Tec EBSD sample holder kits with 20° / 70° pre-tilt angle for Hitachi SEMs and the versatile EM-Tec SEM stage adapters

*Prices are without tax. Tax might be added in cart.


EM-Tec TE3 t-EBSD holder kit 20 / 70 for three TEM / FIB Lift-out grids, M4 EM-Tec TE3 t-EBSD holder kit 20 / 70 for three TEM / FIB Lift-out grids, M4
Artikel # Einheit Preis* Bestellung / Anfrage
12-003273 each €480,50
Qty:



EM-Tec TE1 t-EBSD holder kit 20 / 70 for single TEM / FIB Lift-out grid, M4 EM-Tec TE1 t-EBSD holder kit 20 / 70 for single TEM / FIB Lift-out grid, M4
Artikel # Einheit Preis* Bestellung / Anfrage
12-003271 each €325,50
Qty:






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